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Fabrication of MoS2 microflowers for hydrogenation of nitrobenzene
Li, Zhongcheng1,2; Zhang, Deliang1; Ma, Jiaojiao1; Wang, Debao1; Xie, Congxia1
2018-02-15
Source PublicationMATERIALS LETTERS
ISSN0167-577X
Volume213Pages:350-353
Corresponding AuthorLi, Zhongcheng(zhongchengli@qust.edu.cn) ; Wang, Debao(swang@qingdaonews.com) ; Xie, Congxia(xiecongxia@126.com)
AbstractMoS2 microflowers with the size of 3.9-5.8 mu m in diameter, which is constructed by nanosheets, are hydrothermally synthesized using sodium diethyldithiocarbamate trihydrate as the sulfur source. Studies on the hydrothermal process reveal that the temperature plays crucial roles in determining the crystal phase of MoS2. It is found that the higher temperature favors the reduction of Mo (VI) to Mo (IV). The obtained MoS2 microflowers are highly active and selective for hydrogenation of nitrobenzene into aniline. Compared with commercial MoS2, the higher percentage of coordinative unsaturated Mo sites on MoS2 microflowers offer a relatively higher catalytic activity. (c) 2017 Elsevier B.V. All rights reserved.
KeywordMoS2 microflowers Coordinative unsaturated Mo sites Nitrobenzene hydrogenation Functional Microstructure
DOI10.1016/j.matlet.2017.11.042
WOS KeywordTEMPERATURE-PROGRAMMED REDUCTION ; NITROARENES ; HYDRODESULFURIZATION ; NANOPARTICLES ; CATALYSTS
Indexed BySCI
Language英语
Funding ProjectNational Natural Science Foundation of China[21503117] ; National Natural Science Foundation of China[31270615] ; project of Shandong Province Higher Educational Science and Technology Program[J16LC16] ; Key Laboratory of Renewable Energy, Chinese Academy of Sciences[Y607k81001] ; Natural Science Foundation of Shandong Province[ZR2017MB034]
WOS Research AreaMaterials Science ; Physics
Funding OrganizationNational Natural Science Foundation of China ; project of Shandong Province Higher Educational Science and Technology Program ; Key Laboratory of Renewable Energy, Chinese Academy of Sciences ; Natural Science Foundation of Shandong Province
WOS SubjectMaterials Science, Multidisciplinary ; Physics, Applied
WOS IDWOS:000419049300088
PublisherELSEVIER SCIENCE BV
Citation statistics
Cited Times:6[WOS]   [WOS Record]     [Related Records in WOS]
Document Type期刊论文
Identifierhttp://ir.giec.ac.cn/handle/344007/22559
Collection中国科学院广州能源研究所
Corresponding AuthorLi, Zhongcheng; Wang, Debao; Xie, Congxia
Affiliation1.Qingdao Univ Sci & Technol, Coll Chem & Mol Engn, State Key Lab Base Ecochem Engn, Qingdao 266042, Peoples R China
2.Chinese Acad Sci, Guangzhou Inst Energy Convers, CAS Key Lab Renewable Energy, Guangzhou 510640, Guangdong, Peoples R China
First Author AffilicationGuangZhou Institute of Energy Conversion,Chinese Academy of Sciences
Recommended Citation
GB/T 7714
Li, Zhongcheng,Zhang, Deliang,Ma, Jiaojiao,et al. Fabrication of MoS2 microflowers for hydrogenation of nitrobenzene[J]. MATERIALS LETTERS,2018,213:350-353.
APA Li, Zhongcheng,Zhang, Deliang,Ma, Jiaojiao,Wang, Debao,&Xie, Congxia.(2018).Fabrication of MoS2 microflowers for hydrogenation of nitrobenzene.MATERIALS LETTERS,213,350-353.
MLA Li, Zhongcheng,et al."Fabrication of MoS2 microflowers for hydrogenation of nitrobenzene".MATERIALS LETTERS 213(2018):350-353.
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