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生物质灰熔融电容测试实验研究
Alternative TitleSTUDY OF BIOMASS ASH MELTING TEST WITH ELECTRIC CAPACITANCE
赖喜锐1,2; 周肇秋1; 刘华财1; 黄艳琴1; 阴秀丽1; 吴创之1
2017-02
Source Publication太阳能学报
ISSN0254-0096
Volume38Issue:2Pages:558-564
Abstract提出一种利用电容测量生物质灰渣熔融状态的方法,以低熔点的玉米芯灰为样品进行测试,并与X射线荧光分析(XRF)、X射线衍射分析(XRD)、热重-差热分析(TG-DSC)结果进行比较.实验结果表明:玉米芯灰样在600-1000℃加热过程中质量的减少主要由灰分中KCl随加热过程挥发所致,并影响灰熔融温度预测结果;灰样烧结温度为800-900℃,电容测试结果为825℃,TG-DSC测试结果为875℃,灰熔点仪测试结果为990℃.电容测量结果与灰样熔融结渣情况一致,电容变化可准确反映灰样相变情况.与常规灰熔点测试和热重分析相比,该方法可实现实时监控测量,并减小测试过程中碱金属元素受热挥发造成的误差.
Other AbstractA novel method for biomass ash melting measurement with electric capacitance was proposed. The melting process of corncob ash with relatively low melting point was investigated, and the measuring result was compared with that determined by X-ray fluorescence analysis (XRF) , X-ray diffraction analysis (XRI)) and thermogravimetric- differential scanning calorimeter (TG-DSC). The results show that the ash mass decreases while heated under 600-1000 ℃ due to the volatilization of KC1, which would influence the estimation of ash fusion temperature. The corncob ash melting temperature ranging from 800 ℃ to 900 ℃ was measured to be 825 ℃ by this method, 875 ℃ by TG-DSC, and 990 ℃ by ash melting point apparatus, respectively. Having the same changing tendency with the ash melting process, the variation of electric capacitance could accurately reflect the phase change of ash. Compared with common melting point measurement and TG-DSC, this method can be used for real-time monitoring with less errors caused by volatilization of alkali metals.
Keyword生物质灰 熔融 电容测试 XRF XRD TG-DSC biomass ash melting electric capacitance measurement XRF XRD TG-DSC
Language中文
Document Type期刊论文
Identifierhttp://ir.giec.ac.cn/handle/344007/16655
Collection中国科学院广州能源研究所
Corresponding Author周肇秋
Affiliation1.中国科学院广州能源研究所,中国科学院可再生能源重点实验室,广东省新能源和可再生能源研究开发与应用重点实验室,广州510640;
2.中国科学院大学,北京100049
First Author AffilicationGuangZhou Institute of Energy Conversion,Chinese Academy of Sciences
Recommended Citation
GB/T 7714
赖喜锐,周肇秋,刘华财,等. 生物质灰熔融电容测试实验研究[J]. 太阳能学报,2017,38(2):558-564.
APA 赖喜锐,周肇秋,刘华财,黄艳琴,阴秀丽,&吴创之.(2017).生物质灰熔融电容测试实验研究.太阳能学报,38(2),558-564.
MLA 赖喜锐,et al."生物质灰熔融电容测试实验研究".太阳能学报 38.2(2017):558-564.
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