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p-Hydroxybenzenesulfonic acid-formaldehyde solid acid resin for the conversion of fructose and glucose to 5-hydroxymethylfurfural
Li, Wenzhi1; Zhang, Tingwei1; Xin, Haosheng2; Su, Mingxue3; Ma, Longlong4; Jameel, Hason5; Chang, Hou-min5; Pei, Gang1
2017
Source PublicationRSC ADVANCES
Volume7Issue:44Pages:27682-27688
AbstractA novel solid p-hydroxybenzenesulfonic acid-formaldehyde resin (SPFR) was prepared via a straightforward hydrothermal method. The catalytic properties of SPFR solid acids were evaluated in the dehydration reaction of fructose and glucose to 5-hydroxymethylfurfural (HMF). SEM, TEM, N-2 adsorption-desorption, elemental analysis (EA), thermogravimetric analysis (TGA), and FT-IR were used to explore the effects of catalyst structure and composition on the HMF preparation from fructose. The effects of reaction time and temperature on the dehydration of fructose and glucose were also investigated. An HMF yield as high as 82.6% was achieved from fructose at 140 degrees C after 30 min, and 33.0% was achieved from glucose at 190 degrees C in 30 min. Furthermore, the recyclability of SPFR for the HMF production from fructose in 5 cycles was good.
SubtypeArticle
WOS HeadingsScience & Technology ; Physical Sciences
DOI10.1039/c7ra03155f
WOS Subject ExtendedChemistry
WOS KeywordGAMMA-VALEROLACTONE ; IONIC LIQUID ; CATALYTIC CONVERSION ; BIPHASIC SYSTEM ; LEVULINIC ACID ; MCM-41 SILICA ; LEWIS-ACID ; DEHYDRATION ; BIOMASS ; CHITOSAN
Indexed BySCI
Language英语
Funding OrganizationState Key Program of the National Natural Science Foundation of China(51536009) ; National Key Technology R&D Program of China(2015BAD15B06) ; Science and Technological Fund of the Anhui Province(1508085J01)
WOS SubjectChemistry, Multidisciplinary
WOS IDWOS:000402166600059
Citation statistics
Cited Times:17[WOS]   [WOS Record]     [Related Records in WOS]
Document Type期刊论文
Identifierhttp://ir.giec.ac.cn/handle/344007/14133
Collection中国科学院广州能源研究所
Affiliation1.Univ Sci & Technol China, Dept Thermal Sci & Energy Engn, Hefei 230026, Peoples R China
2.Anhui Jianzhu Univ, Inst Mat & Chem Engn, Hefei 230022, Peoples R China
3.Univ Sci & Technol China, Dept Chem, Hefei 230026, Peoples R China
4.Chinese Acad Sci, Guangzhou Inst Energy Convers, CAS Key Lab Renewable Energy, Guangzhou 510640, Guangdong, Peoples R China
5.North Carolina State Univ, Dept Forest Biomat, Raleigh, NC 27695 USA
Recommended Citation
GB/T 7714
Li, Wenzhi,Zhang, Tingwei,Xin, Haosheng,et al. p-Hydroxybenzenesulfonic acid-formaldehyde solid acid resin for the conversion of fructose and glucose to 5-hydroxymethylfurfural[J]. RSC ADVANCES,2017,7(44):27682-27688.
APA Li, Wenzhi.,Zhang, Tingwei.,Xin, Haosheng.,Su, Mingxue.,Ma, Longlong.,...&Pei, Gang.(2017).p-Hydroxybenzenesulfonic acid-formaldehyde solid acid resin for the conversion of fructose and glucose to 5-hydroxymethylfurfural.RSC ADVANCES,7(44),27682-27688.
MLA Li, Wenzhi,et al."p-Hydroxybenzenesulfonic acid-formaldehyde solid acid resin for the conversion of fructose and glucose to 5-hydroxymethylfurfural".RSC ADVANCES 7.44(2017):27682-27688.
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