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Synthesis and Optical Property of ZnO/SiO2 Nanocomposite Cryogels
Su, Lifen1; Miao, Lei2; Zhang, Ming3; Qian, Jiasheng1; Xia, Ru1; Yang, Bin1; Chen, Peng1
2014-03-01
发表期刊ASIAN JOURNAL OF CHEMISTRY
卷号26期号:5页码:1257-1260
摘要In this paper, ZnO cryogels with a dopant of SiO2 with molar ratio of 9:1 to 1:1 were prepared by sol-gel technology and dried by a novel vacuum freeze drying using a co-precursor method. The as-prepared ZnO/SiO2 nanocomposites were annealed in air at 250, 500 and 800 degrees C for 45 min, respectively. The structure and morphology of the nanocomposites were determined by X-ray diffraction (XRD) and field emission scanning electron microscopy. The optical properties were estimated not only by UV-visible spectrometer but also theoretical calculation. The annealed nanocomposites exhibited hexagonal Wurtzite structure ZnO and whose crystallinity became better as an increase of annealing temperature. The amounts of doping SiO2 affect the optical band gaps and morphology of ZnO/SiO2 nanocomposites significantly. After annealing, the obtained ZnO nanorods grow up in size from the SEM images with annealing temperature ranging from 250 to 500 degrees C and flowerlike ZnO was formed with tetragonal pillars at 800 degrees C.
文章类型Article
关键词Optical Band Gap Zno/sio2 Nanocomposites Cryogels Co-precursor Method
WOS标题词Science & Technology ; Physical Sciences
研究领域[WOS]Chemistry
关键词[WOS]CHEMICAL-SYNTHESIS ; ZNO ; GEL ; NANOSTRUCTURES ; COMPOSITES ; ROUTE
收录类别SCI
语种英语
WOS类目Chemistry, Multidisciplinary
WOS记录号WOS:000335836800001
引用统计
被引频次:1[WOS]   [WOS记录]     [WOS相关记录]
文献类型期刊论文
条目标识符http://ir.giec.ac.cn/handle/344007/10738
专题中国科学院广州能源研究所
作者单位1.Anhui Univ, Anhui Prov Key Lab Environm Friendly Polymer Mat, Coll Chem & Chem Engn, Hefei 230601, Peoples R China
2.Chinese Acad Sci, Key Lab Renewable Energy, Guangzhou Inst Energy Convers, Guangzhou 510640, Guangdong, Peoples R China
3.Yokohama Natl Univ, Dept Phys, Grad Sch Engn, Yokohama, Kanagawa 2408501, Japan
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Su, Lifen,Miao, Lei,Zhang, Ming,et al. Synthesis and Optical Property of ZnO/SiO2 Nanocomposite Cryogels[J]. ASIAN JOURNAL OF CHEMISTRY,2014,26(5):1257-1260.
APA Su, Lifen.,Miao, Lei.,Zhang, Ming.,Qian, Jiasheng.,Xia, Ru.,...&Chen, Peng.(2014).Synthesis and Optical Property of ZnO/SiO2 Nanocomposite Cryogels.ASIAN JOURNAL OF CHEMISTRY,26(5),1257-1260.
MLA Su, Lifen,et al."Synthesis and Optical Property of ZnO/SiO2 Nanocomposite Cryogels".ASIAN JOURNAL OF CHEMISTRY 26.5(2014):1257-1260.
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